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Course Prerequisites: High school algebra Required Textbooks and
Materials
R.R. Reeder, C.D. Schaeffer, Jr., and J.L. Hedrick, “A Manual for General Chemistry Laboratory,” 4th ed., Elizabethtown College, 1987. Laboratory notebook, 60 leaves, quad. ruled. This bound notebook is for your laboratory work only. Safety glasses or goggles for use in laboratory. Prescription eyeglasses are sufficient for use in laboratory, but contact lenses and sunglasses do not meet the requirement and may not be worn. An additional notebook of your own choice for lecture notes. An electronic hand calculator capable of addition, subtraction, multiplication, division, squaring, square root extraction, logarithms, and antilogarithms. Calculators may not be shared during examinations or quizzes. At least one pair of light-weight gloves (such as those commonly available at many grocery stores) is strongly recommended for use in the laboratory. Supplemental Work
Objectives
Chemical Nomenclature &
Calculations Energy in Chemical Systems
In addition to the information
content of each topic, it is important that each student develop the ability
to use that information effectively. Students will be expected to:
Attendance
Problem and Reading Assignments
Examinations and Quizzes
Laboratory
Each laboratory has a faculty instructor and one or more advanced student assistants. When you arrive at the laboratory, one of these people will check your notebook to determine your understanding of the work to be done. He or she will also check to see that you have completed the previous week’s work and that you have submitted your results. If, in the instructor’s opinion, you are unprepared, you will not be permitted to work at that time. If you are behind in laboratory work, you will be told to complete the outstanding work before beginning a new experiment. If you are both prepared and current, you will be signed in and you may conduct your work. The projects must be completed before the end of the period during which they are scheduled. Reports submitted at other times may not be accepted, making you liable to repeat that experiment. Before leaving the laboratory, you must complete the analysis called for at the end of the experiment, and report the results to the instructor. On several occasions noted in the laboratory schedule, you will conduct an experiment in the normal fashion, reflect on your work and method, and then submit a written report on your work. For several of these experiments, you will need to consult with your classmates, discuss with them their results for the same project, and incorporate this information in your report. These formal reports will be graded by the instructor and will contribute to your final course grade. Documentation standards and additional guidance in the preparation of these reports will be provided in class and in laboratory. The laboratory is a very important part of this course. Attendance is required at all sessions. The penalty for any incomplete laboratory work remaining after Friday, April 28, 2006, 2:00 p.m, is failure of the course. Grading
0 - 59%
= F
Final grades will be determined
by combining examination grades (50%), the final examination grade (25%),
a composite of quiz grades (12.5%), and a laboratory evaluation (12.5%
for performance, attendance and reports). Letter equivalents to the
final numerical total are as follows:
Students may request a grade of "I" by submitting a formal written request to the professor of that course. Grades of "I" are assigned for extenuating circumstances only. They are not given simply to allow additional time to complete required course work or to improve a course grade. Forms are available in the Registration & Records Office. Academic Integrity
Disability Statement
Tentative Lecture Outline & Examination Schedule
Reading & Problem Assignments Ch. 1 Reading:
pps. 1 - 34
Ch. 2 Reading:
pps. 41 - 71
Ch. 3 Reading:
pps. 79 - 105
Ch. 4 Reading:
pps. 112 - 146
Ch. 5 Reading:
pps. 154 - 205
Ch. 6 Reading:
pps. 215 - 229
Ch. 11 Reading: pps.
451 - 494
Ch. 12 Reading: pps.504
- 539
Ch. 13 Reading: pps.
548 - 591
Ch. 14 Reading: pps.
598 - 630
Ch. 16 Reading: pps.
697 - 729
Ch. 17 Reading: pps.
737 - 769
Ch. 18 Reading: pps.
775 - 824
Ch. 23 Reading: pps.
1087 - 1130
Tentative Laboratory Schedule
Reminder: The
last date to turn in laboratory data and reports is Friday, April 28, 2:00
p.m. The penalty for any incomplete laboratory work remaining after
this time is failure of the course.
Laboratory Awareness
1. Protective eyewear is required. If glasses are worn, they must have attached side shields. Contact lenses are discouraged and in themselves do not fulfill the requirement. 2. Wear suitable attire (e.g., no shorts or skirts, only closed shoes but no sandals, nonflammable clothing, etc.). Wearing of a lab coat or apron is recommended. Tie back or secure long hair. 3. Know the location and operation of all laboratory safety equipment. Use the fume hoods as much as necessary to minimize the presence of undesirable vapors. Keep your face out of the hood and keep the hood window down as much as possible. If the need to use a safety shower or eyewash station arises, insure sufficient washing or irrigation time and volume to mitigate the problem. Irrigate the contaminated eye until the problem is corrected, making sure that the eyelid is pulled back to expose the eye. If a chemical is spilled on you, wash the area immediately with water. 4. Be familiar with the chemical properties, physical properties, and toxicity of the substances with which you will be working. Ask your instructor to direct you to the location in the chemistry library containing this information. 5. Wear gloves if reagents are toxic, corrosive, or if there is any doubt. 6. Create & maintain a clean and orderly workspace appropriate for the environment and compatible with the experiment in progress. Anticipate the consequences of your actions and plan all work accordingly. It is also your responsibility to insure that your laboratory neighbors act in like fashion. Everyone assists with cleanup at the conclusion of work. 7. Exercise caution when transferring reagents in order to minimize the potential for spills and for contamination of the bulk supply. The incorrect manipulation of container lids is also a common source of contamination. 8. Place waste chemicals in appropriate containers labeled with the contents. Consult an instructor for further details on proper disposal techniques. Place discarded glass only in the special containers designated as such. 9. Use an open flame in this course only when directed to do so. 10. Transport liquids or solids only in closed containers. 11. Always be on the lookout for pressure build-up. Never heat a closed system. When extracting with a separatory funnel, always vent the pressure before and after shaking. It is prudent to begin an extraction in a beaker or a flask where there is plenty of room for gases to escape. 12. Never distill to dryness. 13. Use only round-bottom flasks or filter flasks for evacuation. 14. Use extra caution in manipulating heated objects, especially ironware and glassware. 15. If there is an accident, regardless of how minor, notify the instructor immediately. 16. Eating or drinking is permitted only outside the laboratory. 17. Think while you work and use common sense. Never rush. 18. Perform no unauthorized experiments. 19. Never work alone. 20. Further specialized instruction
will be provided as experimental procedures warrant.
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